Formulation and Evaluation of Herbal Hair Mask
Sonawane Shubham
B*, Sonawane Kalpesh B., Somvanshi D., Sonawane Varun S., Prof. Sayyad Tahir F.
DCS’s A R A College of
Pharmacy, Nagaon, Dhule
*Correspondence: shubhambsonawane17022004@gmail.com; Tel.: +91-9665443060
DOI: https://doi.org/10.71431/IJRPAS.2025.4410
|
Article Information
|
|
Abstract
|
|
Research Article
Received: 21/04/2025
Revised: 23/04/2025
Accepted: 25/04/2025
Published: 30/04/2025
Keywords
Herbal hair mask,
Herbs,
herbal hair oil,
Cosmetics,
Flax seed.
|
|
Hair
care is a vital aspect of personal hygiene and self-presentation, yet many
individuals face issues such as dandruff, hair fall, and dryness due to
stress, hormonal imbalances, poor nutrition, and the frequent use of
chemical-based products. In response, this project presents the development
of a multipurpose herbal hair mask formulated entirely from natural
ingredients. The mask incorporates traditional Ayurvedic components including
castor oil, coconut oil, bhringraj oil, and various herbal extracts such as
neem, basil, and tea tree oil—each selected for their proven benefits in
nourishing the scalp, strengthening hair, and treating dandruff. Designed for
home preparation, the product is safe, affordable, and effective for a range
of hair types, particularly damaged or thinning hair. This formulation
provides a holistic, chemical-free solution that aligns with the rising
global demand for natural and sustainable personal care products.
|
INTRODUCTION
Hair cosmetics can be characterized as
preparations intended for cleaning, altering the texture, changing the color,
revitalizing stressed hair, nourishing the hair, and giving the hair a healthy
appearance. Different people have different varieties of hair; these include
dry hair, oily hair, and regular hair. People these days don't have time to
consider their physical appearance. Issues with hair, split ends, dandruff,
white hair, hair falling out, etc. Stress, scalp infections, hormone
imbalances, insufficient vitamin, food, and mineral intake, and excessive use
of chemical shampoos are the causes of hair problems [1-3].
Nowadays, one of the most crucial
aspects of one's personal life is having a clean scalp and hair. The most vital
component of the body is the hair. Thus, in order to care for them, we developed
a hair mask recipe. The benefits of the components used to the herbal hair mask
for hair are known. The purpose of using a hair mask is to cleanse the hair of
accumulated debris.
The hair mask also contains castor,
coconut, and bhringraj oils, which are applied to the hair. Chemicals are not
used at all in the process of creating hair masks. It doesn't damage your hair
because it solely contains natural components. Hair is a sensitive organ and a
sign of good health. We can assist
hydrate our hair by using an herbal hair mask.
They are very helpful for damaged and dry hair. A hair mask can improve the strength of our hair and the
condition of our scalp. These hair masks are quite helpful, have no
negative effects, and are also manufactured at home. This mask can be made with a variety of substances.
For people with really thin hair or badly damaged hair, this product is quite
helpful. Good hair enhances the attractiveness of our personalities. There are
numerous kinds of masks on the market, however many of them include chemicals.
So, we used herbs to create a product. Making this mask is quite simple.
Because they are readily available, inexpensive, and safe, herbs are frequently
employed as therapeutic agents. The Ayurvedic method was created over 5,000
years ago in India and is still in
use today. There are about 700 prescriptions for medicines
in the Rig Veda and Atharv
Veda. Numerous herbal substances have also been shown
to have good antidandruff activity, including pepper extract, basil extract, neem
extract, rosemary oil, clove oil, coleus oil, and tea tree oil.
The demand for herbal formulations is
rising on the global market. Our project's primary goal was to solve this challenge in its entirety.
Thus, we created a multipurpose herbal antidandruff, conditioning, and
anti-hair fall mask for hair care [4].
MATERIALS AND METHODS
The different parts of the plants were selected for study having
hair care property which is already proven. Following are the ingredients which
we have used in the formulation of hair mask
Table 1. Ingredients
|
Sr. No.
|
Ingredient
|
Biological
Source
|
Constituents
|
Uses
|
|
1.
|
Flax Seeds
|
Linum usitatissimum Linn.
|
Protein, Omega-3- Fatty
Acid, Vit-E
|
For hair Loss & hair
Growth
|
|
2.
|
Neem Powder
|
Azadirachta indica
|
Azadirachta indica, Nimbin, nimbidin,
nimbolide, Flavonoids
|
Increasing the volume of hair
|
|
3.
|
Aloe Vera
|
Aloe perryi
|
Vitamins (A, C, E),
Saponins.
|
Repairs dead skin cells on
the scalp.
|
|
4.
|
Hibiscus Powder
|
Hibiscus rosa-sinensis
|
Saponins, Flavonoids, Tannins.
|
Scalp moisturizer, Treats dandruff and
itching.
|
|
5.
|
Amla Powder
|
Umbelica officinalis
|
Vit. C, Vit. A
|
Strengthens the scalp and hair
|
|
6.
|
Curry Leaves
|
Murraya koenigii
|
Vit. B, Vit C, Essential oil.
|
Promote hair growth, improve scalp health,
and add shine and moisture
|
|
7.
|
Bhringaraj Oil
|
Eclipta prostrata
|
Vit D, Vit E & Keratin
|
Hair Tonic, Nourishment
|
|
8.
|
Coconut Oil
|
Cocous nucifera
|
Triglycerides,
|
Moisturize the hair
|
|
9.
|
Multani Powder
|
Fuller's Earth
|
Silicon dioxide, Aluminium dioxide,
|
Improves blood
circulation,
cleansing
property
|
Pre-formulation
Study
1.
Organoleptic
Properties [1].
Color, Odour, Texture
2.
Physicochemical
Properties [9].
v pH: Measure by using
digital pH meter.
The 1 gm powder was dissolved in 100ml of distilled water and be
sure that all powder is dissolved in the water. Then by using calibrated pH
meter measured the pH value and reported.
v Melting pointy: By using Thiele
tube set up.
Thin-walled capillary melting point
tubes were used to hold melting point of samples. This tube was sealed at one end by using Bunsen
flame. Melting point of hair mask can be determined by introducing a tiny
amount of sample into a small capillary tube attaching this is the stem of a
thermometer centered in a heating bath. Heat the bath slowly and observes the
temperature at which melting starts and complete.
v Solubility: Solubility of substance refers to the amount of substance
that passes into solutions to achieve a saturated solutions at constant
temperature and pressure, 1gm of substance or powdered was weighed accurately
and transfer into a beaker containing 100ml of water This was shaken well and
warmed to increase the solubility then cooled and filter it the residue
obtained is weighed and noted.
Formulation of Herbal Hair mask:
Weighing of ingredients
[4]
All the required ingredients for hair mask
preparation were accurately weighed individually by using digital balance.
Mixing of ingredients [9]
Flaxseeds to the water added in water. Boiled this
water for around 10 minutes and keep string to avoid flaxseeds from sticking to
the base of the utensil. Turned the burner off when you achieve a gel-like
texture neither too dense nor too thin. Let the gel cooled down for about an
hour while it thickens. Put the muslin cloth in a glass measuring cup, and then
empty the gel into it. Now squeezed the gel form the muslin cloth into the
measuring cup in order to strain it, Added the corn Starch to Luke warm water.
Stirred well until smooth and completely dissolved. Put the rest of the water
onto the burner top and bring to Boil.
In a boiling water added the corn starch mixture and
stir continuously. Keep stirring the liquid will change their consistency after
few minutes and start to become more viscous but won’t get the thickness as
required because it happens only after cooling. Stirred until it changes form a
milky white into Vaseline like colour and texture.
RESULT
AND DISCUSSION
Physiochemical properties [9, 14, 15]
Ø pH
The pH of 10% hair mask solution in
distilled water was determined at room temperature 25*C. The pH was measured by
using digital pH meter.
Ø Washability
Formulation was applied on the skin and
ease and extend of washing with water were checked manually.
Ø Nature
of hair after washes
Nature of hair after washes can be done by
collecting the response of volunteers.
Ø Irritancy
Mark the area, on the left-hand dorsal
surface. Then the masked were applied to the area and the time noted. After
interval up to 3hr, it is checked for irritancy effect.
Ø Patch
test
In this procedure, a small amount of
moistened formulation is applied to the hand surface and the effect of the
formulation on irritancy and itching have been noticed.
Table 2: Evaluation parameters of herbal
hair ingredients
|
Ingredients
|
color
|
Odour
|
Taste
|
pH
|
M.P.
|
Solubility
|
|
Curry leaves
powder
|
Green
|
Sulfuryl and
burnt
|
Slightly bitter
and pungent
|
5
|
84*C
|
In soluble
in
oil and water
|
|
Hibiscus
powder
|
pink
|
Pure air
|
Slightly bitter
|
6
|
137*C
|
Soluble in
water
|
|
Neem Leaves
powder
|
Green
|
Sulfur smell
|
Extremely
bitter
|
7
|
80*C
|
Soluble in
water
|
|
Flax seed
|
Brown
|
Nutty smell
|
Mila nutty
flavor
|
7
|
-71*C
|
Insoluble in
water
|
|
Amla powder
|
Brownish
black
|
Acidic
astringent smell
|
Bitter
|
4
|
_
|
Soluble in
water
|
|
Multani
powder
|
Creamy
colour
|
Fresh muddy odour
|
Chalk flavor
|
8
|
_
|
Partially
soluble in water
|
|
Aloe vera Gel
|
White
|
Pungent
|
Bitter
|
5
|
-
|
Souble in
water
|
Table
2 indicate results of evaluation parameter: pH of
curry leaves powder, hibiscus powder, Neem leaves powder, flax seeds, amla
powder, multani powder and aloevera was found to be 5,6,7,7,4,8,5 respectively.
After melting point study, it was observed that curry leaves powder, hibiscus
powder, Neem leaves powder, and flax seed were 84 °C, 137 °C, 80*C and -71 °C
respectively. Hibiscus powder,
Neem leaves powder,
amla powder and aloe vera are soluble
in water. Curry leaves
powder; flax seed were insoluble in water while multani powder
was partially soluble
in water.
Ø
Formulation Study
Table 3: Evaluation of Herbal
Hair Mask
Ø
|
Sr.
No
|
Test
|
Observation
|
|
F1
|
F2
|
F3
|
|
1
|
Colour
|
Brown
|
Brown
|
Greenish brown
|
|
2
|
Nature
|
Semisolid paste
|
Semisolid paste
|
Semisolid paste
|
|
3
|
Odour
|
Unpleasant
|
Pleasant
|
Pleasant
|
|
4
|
Texture
|
Rough
|
Smooth
|
Smooth
|
|
5
|
pH
|
5.2
|
5.6
|
6
|
|
6
|
Washability
|
Not easily
wash
|
Not easily
wash
|
Easily wash
|
|
7
|
Nature of hair
after washes
|
Rough
|
Silky and
smooth
|
Silky and
smooth
|
|
8
|
Viscosity
|
17900mPa.s
|
18500mPa.s
|
18800mPa.s
|
|
9
|
Eye and skin
irritation
|
Present
|
Absent
|
Absent
|
|
10
|
Patch test
|
Present
|
Absent
|
Absent
|
Table 3 indicates result of evaluation parameter was performed to ensure superiority
of prepared herbal hair mask. The formulation of hair mask was prepared and
evaluated for several parameters like colour, odour, nature, texture, pH, washability, eye and skin irritation and patch test. The
colour of formulation was different due to variation in composition of
contents. F1 and F2 are brown in colour and F3 were greenish
brown in colour.
The odour of prepared F3 batch was pleasant in odour.
So, it is good for acceptance. Optimized
batch F3 shows smooth texture.
The pH of all formulation is near to neutral
range. Batch F3 easily washable by using water. After using of herbal hair mask
was provide silky and smooth hair.
Patch test was performed on skin for 24hr
and within this time frame; the area must not come in
contact with water so that is not wash off.
Table 4: Viscosity determination of F3 Herbal
Hair Mask
|
RPM
|
Reading
|
Percentage
|
|
3
|
38000
|
95.0%
|
|
4
|
29970
|
99.9%
|
|
6
|
19960
|
99.8%
|
|
10
|
11980
|
99.8%
|
|
12
|
9650
|
96.5%
|
|
20
|
5304
|
88.4%
|
CONCLUSION
This Study shows the used of herbal
plant products with proven efficacy as in the hair care preparation. Herbal
based cosmetics are popular for their non-toxic nature. Curry leaves flax seeds
Corn starch Hibiscus, Alma powder, coconut oil castor oil and Bhringraj oil
were the herbal ingredients which were used for preparing hair mask Curry leave
which for making hair mask has antidandruff activity which helps to remove the
dandruff hair in very easy manner. Multani powder has a cleansing property
which is an effective cleansing agent. This mask helps to prevents frizzy hair
and giving cooling effects due to the use of castor oil, now Days natural
ingredients are used in more amounts in all over the word due to their safe and
less side effects as compared to chemical-based products. This investigation
was carried out on the basis of traditional and present knowledge that used to
formulate the herbal hair mask to develop few parameters for quality and purity
of herbal hair mask.
CONFLICT
OF INTEREST
Author(s) shall
declare the conflict of interest before submission of manuscript for
publication. The conflict of interest as mentioned in manuscript before
references section. Please note that all articles submitted to the journal will
be evaluated by turnitin for plagiarism.
ACKNOWLEDGEMENT
In general, the
most significant individuals to acknowledge in your acknowledgment are your
research adviser, the principal professor in charge of your project or
research, and any other academic supervisors who are directly involved in your
research. Regardless of how many acknowledgements you have, use the singular
heading.
REFERENCES
1.
Jadhav AP,
Wakale MT, Telangi GM,
Warpe PV. Formulation
and evaluation of herbal anti dandruff hair mask.
International Journal of Scientific Research
in Science and Technology. 2022;9(3):557-564.
2.
Prabha MS, Sravani A, Spandana A, Ramarao N, Aruna MS.
Formulation and Evaluation of herbal hair powder against dandruff.
International journal of Pharmaceutical
Science Review and Research. 2014;28(2):43-473.
3.
Jain U. Beauty through
Herbs. Institute of
Herbal Science
publishers, 1st Edition; c1997,
23-27.
4.
Jaybhaye A, Panchal
R, Nimbalkar
S, Shinde
A, Musmade
D. Formulation
of herbal
hair mask. International
Journal of Creative Research
Thoughts. 2020;8:2480-2485.
5.
Harland DP, Walls RJ, Vernon JA, Dyer JM, Woods JL, Bell F. three-dimensional architecture of microfibrils in human scalp hair cortex. Journal of Structural Biology.
2024;185(3):397-404.
6.
Buffoli B,
Rinaldi F,
Labanca M,
Sorbellini E,
Trink A,
Gunaziroli E,
et al. The
human hair from anatomy to physiology. International Journal of Dermatology. 2014;53(3):331-
341.
7.
Jadhav AV,
Morale D,
Daunderkar A,
Bhujbal N,
Kshirsagar S.
Herbal hair cosmetics:
An overview. World Journal
of Pharmaceutical Science. 2018;6(9):144-152.
8.
Lanjewar A, Maurya S, Sharma
D, Gaur
A. Review
on hair
problem and it’s solution.
Journal of
Drug Delivery and Therapeutics.
2020;10(3):322-329.
9.
Chaughule A,
Zinjad S,
Lokhande R.
Formulation and
evaluation of
protective rule
of flaxseed gel
in hair
growth, nourishment
and anti-dandruff
activity. Journal
of Emerging Technologies and Innovative
Research. 2020;9(6):272-277.
10.
Khristi V, Patel VH. Therapeutic potential of Hibiscus
rosa sinensis. A Review International
Journal of nutrition and Dietecs. 2016;4(2):105-123.
11.
Banerjee PS, Sharma M, Nima RK.
Preparation, evaluation and hair growth
stimulating activity of herbal hair oil. Journal of chemical and Pharmaceutical
Research. 2009;1(1):262-267.
12.
Khile DB.
Review on
hair conditioner
containing curry
leaves, Amla,
Aloe vera,
Neam and flaxseeds.
International Journal
of Creative
Research Thoughts.
2022;10(1):639-640.
13.
Mayurya S, Maury S. A Review on activity on herbal hair mask on hair fall. World
Journal of Pharmaceutical Research. 2022;11(6):316-324.
14.
Ramakrishna S, Gopikrishna UV.
Formulation and evaluation of herbal hair
gel. Scholars International Journal of
Traditional Complementary
Medicine. 2022;5(2):28-22.
15.
Gautam SA, Dwivei SU, Dube KU, Joshi HE.
Formulation and
evaluation of
herbal hair oil.
International Journal of Chemical
Science. 2021;10(1):349-353.