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Sonawane Shubham B*, Sonawane Kalpesh B., Somvanshi D., Sonawane Varun S., Prof. Sayyad Tahir F. Formulation and Evaluation of Herbal Hair Mask. IJRPAS, April 2025; 4 (4): 96-102.

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Formulation and Evaluation of Herbal Hair Mask

Sonawane Shubham B*, Sonawane Kalpesh B., Somvanshi D., Sonawane Varun S., Prof. Sayyad Tahir F.

DCS’s A R A College of Pharmacy, Nagaon, Dhule

 

*Correspondence: shubhambsonawane17022004@gmail.com; Tel.: +91-9665443060

DOI: https://doi.org/10.71431/IJRPAS.2025.4410

Article Information

 

Abstract

Research Article

Received: 21/04/2025

Revised:   23/04/2025

Accepted: 25/04/2025

Published: 30/04/2025

Keywords

Herbal hair mask,

Herbs,

herbal hair oil,

Cosmetics,

Flax seed.

 

Hair care is a vital aspect of personal hygiene and self-presentation, yet many individuals face issues such as dandruff, hair fall, and dryness due to stress, hormonal imbalances, poor nutrition, and the frequent use of chemical-based products. In response, this project presents the development of a multipurpose herbal hair mask formulated entirely from natural ingredients. The mask incorporates traditional Ayurvedic components including castor oil, coconut oil, bhringraj oil, and various herbal extracts such as neem, basil, and tea tree oil—each selected for their proven benefits in nourishing the scalp, strengthening hair, and treating dandruff. Designed for home preparation, the product is safe, affordable, and effective for a range of hair types, particularly damaged or thinning hair. This formulation provides a holistic, chemical-free solution that aligns with the rising global demand for natural and sustainable personal care products.

 

INTRODUCTION

Hair cosmetics can be characterized as preparations intended for cleaning, altering the texture, changing the color, revitalizing stressed hair, nourishing the hair, and giving the hair a healthy appearance. Different people have different varieties of hair; these include dry hair, oily hair, and regular hair. People these days don't have time to consider their physical appearance. Issues with hair, split ends, dandruff, white hair, hair falling out, etc. Stress, scalp infections, hormone imbalances, insufficient vitamin, food, and mineral intake, and excessive use of chemical shampoos are the causes of hair problems [1-3].

Nowadays, one of the most crucial aspects of one's personal life is having a clean scalp and hair. The most vital component of the body is the hair. Thus, in order to care for them, we developed a hair mask recipe. The benefits of the components used to the herbal hair mask for hair are known. The purpose of using a hair mask is to cleanse the hair of accumulated debris.

The hair mask also contains castor, coconut, and bhringraj oils, which are applied to the hair. Chemicals are not used at all in the process of creating hair masks. It doesn't damage your hair because it solely contains natural components. Hair is a sensitive organ and a sign of good health. We can assist hydrate our hair by using an herbal hair mask. They are very helpful for damaged and dry hair. A hair mask can improve the strength of our hair and the condition of our scalp. These hair masks are quite helpful, have no negative effects, and are also manufactured at home. This mask can be made with a variety of substances. For people with really thin hair or badly damaged hair, this product is quite helpful. Good hair enhances the attractiveness of our personalities. There are numerous kinds of masks on the market, however many of them include chemicals. So, we used herbs to create a product. Making this mask is quite simple. Because they are readily available, inexpensive, and safe, herbs are frequently employed as therapeutic agents. The Ayurvedic method was created over 5,000 years ago in India and is still in use today. There are about 700 prescriptions for medicines in the Rig Veda and Atharv Veda. Numerous herbal substances have also been shown to have good antidandruff activity, including pepper extract, basil extract, neem extract, rosemary oil, clove oil, coleus oil, and tea tree oil.

The demand for herbal formulations is rising on the global market. Our project's primary goal was to solve this challenge in its entirety. Thus, we created a multipurpose herbal antidandruff, conditioning, and anti-hair fall mask for hair care [4].

MATERIALS AND METHODS

The different parts of the plants were selected for study having hair care property which is already proven. Following are the ingredients which we have used in the formulation of hair mask

Table 1. Ingredients

Sr. No.

Ingredient

Biological Source

Constituents

Uses

1.

Flax Seeds

Linum usitatissimum Linn.

Protein, Omega-3- Fatty Acid, Vit-E

For hair Loss & hair Growth

2.

Neem Powder

Azadirachta indica

Azadirachta indica, Nimbin, nimbidin, nimbolide, Flavonoids

Increasing the volume of hair

3.

Aloe Vera

Aloe perryi

Vitamins (A, C, E), Saponins.

Repairs dead skin cells on the scalp.

4.

Hibiscus Powder

Hibiscus rosa-sinensis

Saponins, Flavonoids, Tannins.

Scalp moisturizer, Treats dandruff and itching.

5.

Amla Powder

Umbelica officinalis

Vit. C, Vit. A

Strengthens the scalp and hair

6.

Curry Leaves

Murraya koenigii

Vit. B, Vit C, Essential oil.

Promote hair growth, improve scalp health, and add shine and moisture

7.

Bhringaraj Oil

Eclipta prostrata

Vit D, Vit E & Keratin

Hair Tonic, Nourishment

8.

Coconut Oil

Cocous nucifera

Triglycerides,

Moisturize the hair

9.

Multani Powder

Fuller's Earth

Silicon dioxide, Aluminium dioxide,

Improves blood circulation,

cleansing property

 

Pre-formulation Study

1.      Organoleptic Properties [1].

Color, Odour, Texture

2.      Physicochemical Properties [9].

v pH: Measure by using digital pH meter.

The 1 gm powder was dissolved in 100ml of distilled water and be sure that all powder is dissolved in the water. Then by using calibrated pH meter measured the pH value and reported.

v  Melting pointy: By using Thiele tube set up.

Thin-walled capillary melting point tubes were used to hold melting point of samples. This tube was sealed at one end by using Bunsen flame. Melting point of hair mask can be determined by introducing a tiny amount of sample into a small capillary tube attaching this is the stem of a thermometer centered in a heating bath. Heat the bath slowly and observes the temperature at which melting starts and complete.

v    Solubility: Solubility of substance refers to the amount of substance that passes into solutions to achieve a saturated solutions at constant temperature and pressure, 1gm of substance or powdered was weighed accurately and transfer into a beaker containing 100ml of water This was shaken well and warmed to increase the solubility then cooled and filter it the residue obtained is weighed and noted.

Formulation of Herbal Hair mask:

Weighing of ingredients [4]

All the required ingredients for hair mask preparation were accurately weighed individually by using digital balance.

Mixing of ingredients [9]

Flaxseeds to the water added in water. Boiled this water for around 10 minutes and keep string to avoid flaxseeds from sticking to the base of the utensil. Turned the burner off when you achieve a gel-like texture neither too dense nor too thin. Let the gel cooled down for about an hour while it thickens. Put the muslin cloth in a glass measuring cup, and then empty the gel into it. Now squeezed the gel form the muslin cloth into the measuring cup in order to strain it, Added the corn Starch to Luke warm water. Stirred well until smooth and completely dissolved. Put the rest of the water onto the burner top and bring to Boil.

In a boiling water added the corn starch mixture and stir continuously. Keep stirring the liquid will change their consistency after few minutes and start to become more viscous but won’t get the thickness as required because it happens only after cooling. Stirred until it changes form a milky white into Vaseline like colour and texture.

RESULT AND DISCUSSION

Physiochemical properties [9, 14, 15]

Ø  pH

The pH of 10% hair mask solution in distilled water was determined at room temperature 25*C. The pH was measured by using digital pH meter.

Ø  Washability

Formulation was applied on the skin and ease and extend of washing with water were checked manually.

Ø  Nature of hair after washes

Nature of hair after washes can be done by collecting the response of volunteers.

Ø  Irritancy

Mark the area, on the left-hand dorsal surface. Then the masked were applied to the area and the time noted. After interval up to 3hr, it is checked for irritancy effect.

Ø  Patch test

In this procedure, a small amount of moistened formulation is applied to the hand surface and the effect of the formulation on irritancy and itching have been noticed.

Table 2: Evaluation parameters of herbal hair ingredients

 

Ingredients

color

Odour

Taste

pH

M.P.

Solubility

Curry leaves

powder

Green

Sulfuryl and

burnt

Slightly bitter

and pungent

5

84*C

In soluble in

oil and water

Hibiscus

powder

pink

Pure air

Slightly bitter

6

137*C

Soluble in

water

Neem Leaves

powder

Green

Sulfur smell

Extremely

bitter

7

80*C

Soluble in

water

Flax seed

Brown

Nutty smell

Mila nutty

flavor

7

-71*C

Insoluble in

water

Amla powder

Brownish

black

Acidic

astringent smell

Bitter

4

_

Soluble in

water

Multani powder

Creamy colour

Fresh muddy odour

Chalk flavor

8

_

Partially

soluble in water

Aloe vera Gel

White

Pungent

Bitter

5

-

Souble in

water

 

Table 2 indicate results of evaluation parameter: pH of curry leaves powder, hibiscus powder, Neem leaves powder, flax seeds, amla powder, multani powder and aloevera was found to be 5,6,7,7,4,8,5 respectively. After melting point study, it was observed that curry leaves powder, hibiscus powder, Neem leaves powder, and flax seed were 84 °C, 137 °C, 80*C and -71 °C respectively. Hibiscus powder, Neem leaves powder, amla powder and aloe vera are soluble in water. Curry leaves powder; flax seed were insoluble in water while multani powder was partially soluble in water.

Ø  Formulation Study

Table 3: Evaluation of Herbal Hair Mask

Ø   

Sr. No

Test

Observation

F1

F2

F3

1

Colour

Brown

Brown

Greenish brown

2

Nature

Semisolid paste

Semisolid paste

Semisolid paste

3

Odour

Unpleasant

Pleasant

Pleasant

4

Texture

Rough

Smooth

Smooth

5

pH

5.2

5.6

6

6

Washability

Not easily wash

Not easily wash

Easily wash

7

Nature   of   hair

after washes

Rough

Silky and

smooth

Silky and

smooth

8

Viscosity

17900mPa.s

18500mPa.s

18800mPa.s

9

Eye    and    skin

irritation

Present

Absent

Absent

10

Patch test

Present

Absent

Absent

 

Table 3 indicates result of evaluation parameter was performed to ensure superiority of prepared herbal hair mask. The formulation of hair mask was prepared and evaluated for several parameters like colour, odour, nature, texture, pH, washability, eye and skin irritation and patch test. The colour of formulation was different due to variation in composition of contents. F1 and F2 are brown in colour and F3 were greenish brown in colour. The odour of prepared F3 batch was pleasant in odour. So, it is good for acceptance. Optimized batch F3 shows smooth texture. The pH of all formulation is near to neutral range. Batch F3 easily washable by using water. After using of herbal hair mask was provide silky and smooth hair. Patch test was performed on skin for 24hr and within this time frame; the area must not come in contact with water so that is not wash off.

Table 4: Viscosity determination of F3 Herbal Hair Mask

 

RPM

Reading

Percentage

3

38000

95.0%

4

29970

99.9%

6

19960

99.8%

10

11980

99.8%

12

9650

96.5%

20

5304

88.4%

 

CONCLUSION

This Study shows the used of herbal plant products with proven efficacy as in the hair care preparation. Herbal based cosmetics are popular for their non-toxic nature. Curry leaves flax seeds Corn starch Hibiscus, Alma powder, coconut oil castor oil and Bhringraj oil were the herbal ingredients which were used for preparing hair mask Curry leave which for making hair mask has antidandruff activity which helps to remove the dandruff hair in very easy manner. Multani powder has a cleansing property which is an effective cleansing agent. This mask helps to prevents frizzy hair and giving cooling effects due to the use of castor oil, now Days natural ingredients are used in more amounts in all over the word due to their safe and less side effects as compared to chemical-based products. This investigation was carried out on the basis of traditional and present knowledge that used to formulate the herbal hair mask to develop few parameters for quality and purity of herbal hair mask.

CONFLICT OF INTEREST

Author(s) shall declare the conflict of interest before submission of manuscript for publication. The conflict of interest as mentioned in manuscript before references section. Please note that all articles submitted to the journal will be evaluated by turnitin for plagiarism.

ACKNOWLEDGEMENT

In general, the most significant individuals to acknowledge in your acknowledgment are your research adviser, the principal professor in charge of your project or research, and any other academic supervisors who are directly involved in your research. Regardless of how many acknowledgements you have, use the singular heading.

REFERENCES       

1.                    Jadhav AP, Wakale MT, Telangi GM, Warpe PV. Formulation and evaluation of herbal anti dandruff hair mask. International Journal of Scientific Research in Science and Technology. 2022;9(3):557-564.

2.                    Prabha MS, Sravani A, Spandana A, Ramarao N, Aruna MS. Formulation and Evaluation of herbal hair powder against dandruff. International journal of Pharmaceutical Science Review and Research. 2014;28(2):43-473.

3.                    Jain U. Beauty through Herbs. Institute of Herbal Science publishers, 1st Edition; c1997, 23-27.

4.                    Jaybhaye A, Panchal R, Nimbalkar S, Shinde A, Musmade D. Formulation of herbal hair mask. International Journal of Creative Research Thoughts. 2020;8:2480-2485.

5.                    Harland DP, Walls RJ, Vernon JA, Dyer JM, Woods JL, Bell F. three-dimensional architecture of microfibrils in human scalp hair cortex. Journal of Structural Biology. 2024;185(3):397-404.

6.                    Buffoli B, Rinaldi F, Labanca M, Sorbellini E, Trink A, Gunaziroli E, et al. The human hair from anatomy to physiology. International Journal of Dermatology. 2014;53(3):331- 341.

7.                    Jadhav AV, Morale D, Daunderkar A, Bhujbal N, Kshirsagar S. Herbal hair cosmetics: An overview. World Journal of Pharmaceutical Science. 2018;6(9):144-152.

8.                    Lanjewar A, Maurya S, Sharma D, Gaur A. Review on hair problem and it’s solution. Journal of Drug Delivery and Therapeutics. 2020;10(3):322-329.

9.                    Chaughule A, Zinjad S, Lokhande R. Formulation and evaluation of protective rule of flaxseed gel in hair growth, nourishment and anti-dandruff activity. Journal of Emerging Technologies and Innovative Research. 2020;9(6):272-277.

10.            Khristi V, Patel VH. Therapeutic potential of Hibiscus rosa sinensis. A Review International Journal of nutrition and Dietecs. 2016;4(2):105-123.

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